Patent Intelligence / US 6,774,146 B2
US 6,774,146 B2

Dispersant and foaming agent combination

Pairs a naphthalene-sulfonate–formaldehyde dispersant with a defined molecular-weight window (MW 17 000 – 47 000) with an alkyl / alkyl-ether sulfate soap, so that air is entrained more efficiently and board weight drops without losing strength.

Dispersant + surfactant system
Assignee
Geo Specialty Chemicals Inc
Inventors
Arpad Savoly, Dawn P. Elko, Bennie Veal, James McCrary
Jurisdiction
United States (USPTO)
Filed
2002-08-07
Published
2004-08-10
Priority
2002-08-07
Fig. · Dispersant molecular-weight window
claim 1 · 17 000 – 47 000 g/mol
MW claim window10k20k30k40k50kweight-average molecular weight (g/mol)SOAP COMPONENTalkyl sulfate + alkyl-ether sulfate→ entrains air, lowers core density
Schematic illustration by Nordgyp Labs — not a reproduction of the patent drawings. Values reflect claims/abstract as filed.
Fig. · Where in the line this patent acts
stage highlight
QuarryCalcinationStucco siloMixerACTS HEREForming tableSetting beltKilnCut & bundling
Schematic illustration by Nordgyp Labs. Stages are a simplified reference layout — real plant topologies vary.
Why this patent matters

Dispersants and foaming agents are usually developed separately: the chemistry team picks a dispersant for water reduction, and process picks a foamer for entrained air. This patent argues that the two are actually coupled — the MW distribution of the NS-formaldehyde polymer changes how the soap behaves at the air-water interface.

How the claim works
  1. 01The dispersant is a naphthalene-sulfonate–formaldehyde alkali-salt polymer restricted to a weight-average molecular weight of 17 000 to 47 000 g/mol.
  2. 02The foaming agent is a soap combining an alkyl sulfate and an alkyl-ether sulfate (both alkali salts).
  3. 03Together, according to the patent, the pair entrains air more efficiently — meaning more void volume for the same soap dose — which lowers total board weight without a matching loss of core strength.
Key parameters — verbatim from the record
ParameterValueSource
Dispersant typenaphthalene-sulfonate–formaldehyde alkali-salt polymerclaim 1
Dispersant weight-average MW window≈ 17 000 – 47 000 g/molclaim 1
Foaming agentmixture of alkyl sulfate + alkyl-ether sulfate (alkali salts)claim 1
What this means on the plant floor
  • 01When qualifying a new dispersant lot, MW distribution — not only sulphonate content or solids — should be part of incoming-goods testing.
  • 02A change of soap supplier can invalidate a stable dispersant/foam pair even when the new soap looks identical on paper. This patent is a good reference when troubleshooting sudden density drift after a supplier change.
Abstract — verbatim from Google Patents

The present invention provides a dispersant and foaming agent combination that is useful in the production of gypsum wallboard and other aqueous cementitious products. The dispersant in the combination according to the invention is a naphthalene sulfonate-aldehyde condensate alkali salt polymer having a weight average molecular weight of from about 17,000 to about 47,000. The alkali is preferably an alkali metal and/or an alkaline earth metal. The aldehyde is preferably formaldehyde. The foaming agent used in the combination according to the invention is a soap, preferably an alkali salt of an alkyl ether sulfate and/or an alkyl sulfate. The combination of a high molecular weight dispersant and a foaming agent produces a gypsum wallboard core effect that more efficiently entrains air (i.e., creates void space), thereby lowering overall board weight without detrimentally affecting strength.

Claim 1 — verbatim

A dispersant and foaming agent combination for use in the production of gypsum wallboard comprising: a naphthalene sulfonate-aldehyde condensate alkali salt polymer having a weight average molecular weight from about 17,000 to about 47,000; and a soap; wherein the aldehyde in the naphthalene sulfonate-aldehyde condensate alkali salt polymer is formaldehyde and the soap comprises a mixture of an alkyl sulfate and an alkyl ether sulfate.

Further claims, drawings, prosecution history and legal status: see the official record.

Sources
  1. [1]US 6,774,146 B2 — Dispersant and foaming agent combination Google Patents · 2004-08-10